Synthesis, Spectroscopic Studies and X-Ray Crystal Structure of

Journal Article
, H. Z. Alkhathlan, M. A. Al-Jaradah, K. A. Al-Farhan and A. A. Mousa . 2004
نوع عمل المنشور: 
بحث
المجلة \ الصحيفة: 
Phosphorus, Sulfur and Silicon, 2004, 179, 1
رقم العدد: 
1
الصفحات: 
179
مستخلص المنشور: 

 
Abstract
N-[2-(œ-Bromoacetyl)phenyl]imides (prepared in two steps from 2-aminoacetophenone) gave upon treatment with sodium azide fused azidoquinolines via an intamolecular cyclization. Reaction of the above azides with phosphines gave N-heteryliminophosphoranes. The IR, 1H-, 13C-, and 31P-NMR and MS spectra of these compounds as well as the X-ray crystal structure of two of them is reported