Al–TiC nanocomposite materials have been prepared by a new in situ synthesizing technique. A mixture of aluminum, titanium, and graphite has been prepared using ball milling technique and then melted in a high frequency induction heat furnace (HFIHF) at different sintering temperatures, namely 900, 1100, and 1300 ° C. The effect of sintering temperature on the corrosion of the Al–TiC composite in 3.5% NaCl solutions was investigated using cyclic potentiodynamic polarization, chronoamperometric current-time, open-circuit potential, and electrochemical impedance spectroscopy measurements.