dvanced electrocatalysts for the fabrication of sustainable hydrogen from water splitting are innermost to energy research. Herein, we report the growth of iron diselenide (FeSe2) nanorods on graphene oxide (GO) sheets using two-step process viz., simple hydrothermal reduction and followed by wet chemical process. The orthorhombic phase of FeSe2 incorporated GO nanosheet was developed as a low-cost and efficient electrocatalyst for hydrogen evolution reaction (HER) by water splitting.

Herein, we have prepared different weight percentages of (10%, 20% and 30%) of α-FeOOH on BiOI visible light active α-FeOOH/BiOI nanocomposite via facile wet impregnation method. The rod-like morphology of α-FeOOH and flake-like morphology of BiOI photocatalyst were fabricated via hydrothermal process. The synthesized photocatalyst were explored by different characterization methods such as FT-IR, XRD, FE-SEM, EDAX, HR-TEM and UV–vis DRS. The photocatalytic behavior was assessed by the photodegradation of Rhodamine B (RhB) under visible-light illumination.

Photoelectrochemical water splitting with metal oxide semiconductors offers a cost-competitive alternative for the generation of solar fuels. Most of the materials studied so far suffer from poor charge-transfer kinetics at the semiconductor/liquid interface, making compulsory the use of catalytic layers to overcome the large overpotentials required for the water oxidation reaction. Herein, we report a very soft electrolytic synthesis deposition method, which allows remarkably enhanced water oxidation kinetics of BiVO4 photoanodes by the sequential addition of Zr and Fe precursors.

The electrochemical method of producing hydrogen peroxide using a titanium oxide nanotube catalyst is an electrochemical process for producing hydrogen peroxide using a cathode formed as a nanostructured titania (TiO2) electrode surface treated with nitrogen. An anode and the cathode are immersed in an alkaline solution saturated with oxygen in an electrolytic cell. An electrical potential is established across the cathode and the anode to initiate electrochemical reduction of the oxygen in the alkaline solution to produce hydrogen peroxide dissolved in the alkaline solution.